X 光繞射儀 X-ray Diffraction System

聯絡方式 Contact

儀器管理者 Instrument administrator

賴良一先生 Mr. Rax Lai TEL: 03-5712121 ext 55637

EMAIL: rexlai@nycu.edu.tw

對外開放服務時間 Opening hours

週一~週五 08:30~17:00

08:30~17:00 from Monday to Friday.

使用功能說明 Applications

1. Poly-crystal s, crystal and phase identification (θ-2θ 、 θ scan)

2. Thin film diffraction and grazing incident x-ray diffraction

3. Powder, bulk diffraction and rocking curve

4. Small area diffraction

規格 Specifications

1.Brand 1 ： PANalytical, Model AERIS (40KV ， 7.5mA)

2.Sealed Tube ：全功率 1100W

3.光學系統包含(Optical system contains)： Soller slit、 Graphite monochromator、 Dual channel analyzer crystal 、 Double crystal (1 st and 2 nd crystal channel cut)

4.解析度(Resolution)： 5 、 12 、 25 arcsec depend on the channel cut

收費標準 Fee

	委託操作費用 Commissioning fee	自行操作會員收費 independent-operation fee	自行操作訓練費Training fee
學術單位Academic institute	NT$1500元/sample	Not available	Not available
業界Corporation	NT$3000元/sample	Not available	Not available

若由各單位合格操作者自行訓練，其訓練使用時數由各單位之自行操作會員時數扣除費用

若委託本中心代為訓練，費用為表格中自行操作訓練費

If training is conducted by a qualified operator, the charge for the training period will be deducted from the membership account of the institute. If the training is conducted by the administrator, the charge is referred to the table.

管理及服務辦法 User regulations

1.本機台為B級機台，提供委託及自行操作服務。

The system is classified as a Grade A instrument, and operation can be carried out by the individual making the reservation or by qualified personnel.

2.申請委託操作者須事先與儀器管理員連絡並進行實驗討論評估，確認樣品及製程可使用本機台，並由管理員估價計算費用後，經指導教授或主管同意後，方可提出使用申請。

Those applying for commissioned operation should discuss and evaluate the experiment with the instrument administrator in advance, ensuring that the sample and fabrication process are suited for the instrument. The application can be filed after the cost is estimated by the administrator and approved by either the advisor or the supervisor.

3.委託操作使用者採序號預約，確認可提出使用申請者請先至本中心網站下載『實驗申請單』，詳填資訊後，e-mail至cnst-adm@cc.nctu.edu.tw並以電話或E-mail與儀器負責人洽詢使用時段及確認實驗條件與試片製備。委託申請人需在現場共同進行實驗。

Each case of commissioned operation is by reservation only. Applicants who have been evaluated and approved can down the “ application form” from our website, and email the completed form to cnst-adm@cc.nctu.edu.tw. The applicants are required to contact the instrument supervisor via phone or email regarding the available time slot, sample preparation and fabrication. The applicants have to be present for the duration of the experiment.

4.使用者須遵守實驗室所有相關規定。違反實驗室規定者依本中心實驗室管理規則辦理。

Users must abide by the regulations of the laboratory. Those in violation of lab regulations are subject to punishments accordingly.

5.如有任何疑問，歡迎來電洽詢儀器負責人員。

Please feel free to contact the administrator for any further inquiries.

6.機台使用費用規定請參照『收費標準』。

Please refer to “Fee” for details of fees for using the instrument.

自行操作訓練與考核辦法 Guideline for independent operation and evaluation

樣品規範 Sample specifications

1.使儀器提供給必要研究者使用，避免儀器資源的浪費，建議與機台管理者詳細討論後，再決定是否進入機台觀察，以充分發揮本儀器之功能。

Use of instruments should be prioritized for researchers requiring the instruments. To avoid any possible waste of resources, users must discuss with the administrator before deciding whether observation is necessary. Usage of the machine should be optimized.

2.存取資料請自備空白光碟片。為避免設備中毒，禁用隨身碟進行資料傳輸。

Users are advised to prepare CDs for data storage. The use of flash drive is forbidden to prevent any possibility of virus infection.

3.自行操作人員，若擅自放入上述有害的試樣於本儀器者，將被吊銷操作資格。

If the qualified user is found loading any harmful sample with above-mentioned description, the user will be disqualified from operating the instrument.

4.委託操作者上機前，技術員會再次要求確認您的樣品種類，請誠實申報。若發現申報不實，本中心將取消您的使用資格。

In cases of commissioned operation, the administrator will verify the description of the sample with you. If sample description is found to be false, you will be disqualified from using the instrument.

5.若因違反規定造成儀器污染或損壞時，所隸屬單位及其指導教授須負責賠償，賠償費用由原廠評估，再由本中心開會決議後執行並暫停儀器之使用權。

If violation of regulation results in contamination or damage of the instrument, the institute and the advisor will bear the cost of compensation, which will be estimated by the manufacturer. We may disqualify the user from using the instrument.