傅氏紅外線光譜儀 Fourier Transform Infrared Spectrometer

聯絡方式 Contact

儀器管理者 Instrument administrator

李良箴博士Dr. L. C. Li

TEL: 03-5712121 ext 55634

EMAIL: lcli@nycu.edu.tw

對外開放服務時間 Opening hours

週一~週日上午8:00~晚上24:00。
8:00~24:00 from Monday to Sunday.

使用功能說明 Applications

1. Reflection spectrum

2. Transmission spectrum

規格 Specifications

Frequency range:

Mid-IR: 700-7899 cm^-1

Resolution: 5 cm^-1

Operating vacuum: 3 mbar

Source: globar

Beamsplitter: KBr beamsplitter

Detector: DTGS detector with a KBr window

Measurement modules: Transmission and reflection modules (aperture of sample holder = 7 mm)

收費標準 Fee

1. 委託操作費用 (Commissioning fee)

學術單位(Academic institute): NT$1700 / hr

會員(Membership): NT$28000 / 20hrs；NT$48000 / 40hrs

業界(Corporation): NT$3400 / hr

2. 自行操作會員收費 (independent-operation fee)

學術單位 (Academic institute): NT$700 / hr

會員(Membership): NT$14000 / 20hrs；NT$24000 / 40hrs

業界(Corporation): No service

3. 自行操作訓練(Training fee)

若由各單位合格操作者自行訓練，其訓練使用時數由各單位之會員時數扣除費用。若委託本中心代為訓練，費用為：

If training is conducted by a qualified operator, the charge for the training period will be deducted from the membership account of the institute. If the training is conducted by the administrator, the charge is as follows:

學術單位(Academic institute): NT$20000 / 10 hours (2000 / hr)

管理及服務辦法 User regulations

1. 本機台為B級機台，提供委託及自行操作服務。
The system is classified as a Grade B instrument, and operation can be carried out by the individual making the reservation or by qualified personnel.

2. 申請委託操作者須事先與儀器管理員連絡並進行實驗討論評估，確認樣品及製程可使用本機台，並由管理員估價計算費用後，經指導教授或主管同意後，方可提出使用申請。

Those applying for commissioned operation should discuss and evaluate the experiment with the instrument administrator in advance, ensuring that the sample and fabrication process are suited for the instrument. The application can be filed after the cost is estimated by the administrator and approved by either the advisor or the supervisor.

3. 委託操作使用者採序號預約，確認可提出使用申請者請先至本中心網站下載『FTIR實驗申請單』，詳填資訊後，e-mail至cnst-adm@cc.nctu.edu.tw並以電話或E-mail與儀器負責人洽詢使用時段及確認實驗條件與試片製備。委託申請人需在現場共同進行實驗。

Each case of commissioned operation is by reservation only. Applicants who have been evaluated and approved can down the “FTIR application form” from our website, and email the completed form to cnst-adm@cc.nctu.edu.tw. The applicants are required to contact the instrument administrator via phone or email regarding the available time slot, sample preparation and fabrication. The applicants have to be present for the duration of the experiment.

4. 申請人按通知時間至實驗室做光路調校及試片測試。

The applicant will be informed the time for calibration of optical path and measurement. Please arrive the lab on time.

5. 由於實驗操作(如控溫等過程)有其所需之時間，會視實驗者狀況調整時間，故只能按預約順序排序，無法確定等候時間長短。

Because some experimental procedures, such as temperature control, can not be interrupted, the ending time of the experiment is not predictable. The process of the measurement will be adjusted according to the progress of the experiment. The reservation will be in the order of reserved number. The exact timetable is not available.

6. 使用者須遵守實驗室所有相關規定。違反實驗室規定者依本中心實驗室管理規則辦理。

Users must abide by the regulations of the laboratory. Those in violation of lab regulations are subject to punishments accordingly.

7. 如有任何疑問，歡迎來電洽詢儀器負責人員。

Please feel free to contact the administrator for any further inquiries.

8. 機台使用費用規定請參照『收費標準』。

Please refer to “Fee” for details of fees for using the instrument.

自行操作訓練與考核辦法 Guideline for independent operation and evaluation

1. 本系統自行操作以指導教授、計畫主持人或公司行號為單位，每位申請者須同時提出其研究使用計畫及材料特性予本中心，由本中心評估並決定是否可接受其申請。

The applicants who want to operate by themselves need to submit the details of their experiment and sample material for application of membership and the training program. The account of membership is registered under your supervisor, PI, or company name.

2. 申請者上網下載並填寫『FTIR實驗申請單』詳填使用者與試片資訊後，e-mail至lcli@faculty.nctu.edu.tw，本中心將儘速回覆您的使用申請。申請核可後，管理員會以E-mail將『見習訓練紀錄表』寄予申請人，在申請人見習時數完成後，可email與管理員洽詢上機訓練時段。

Applicants should download the “FTIR application form” online and email the completed form, including details about the user and lamella, to lcli@faculty.nctu.edu.tw. We will respond to your application as soon as possible. Once the application is approved, the administrator will email a log sheet for the probationary training to the applicant. Upon completion of probationary training, the applicant can contact the administrator for the booking of hands-on training.

3. 自行操作分為部份自行操作者與全程自行操作者。部份自行操作者僅可操作量測儀器端之系統，並不包括整體儀器環境操作。而全程自行操作者則為已受過適當操作訓練之使用者，由本中心評估並決定是否接受訓練申請。

There are two kind of independent operation licenses: partially and fully operating users. For partially operating users, they are only allowed to operate the measuring system. Controlling the cryogenic chamber and adjusting optical system are forbidden. Those applying the fully operating user license need to be go through properly hands-on training after they have the partially operating user license.The rights of permission for fully operating user training is reserved.

4. 本機台訓練時數其規定如下：部份自行操作新訓人員累積訓練時數達 10hr以上者方可向儀器負責人申請考核。全程自行操作新訓人員需會累積測量訓練時數達 10hr以上及所有儀器操作時數達20hr以上者，方可向儀器負責人申請考核。

The regulations of training program are: For the partially operating license, the user has to accumulate 10 hours of hands-on training before applying for qualification. Once the user accumulates over 10 hours of partially independent operation, he may apply for the hands-on fully operating training. After accumulating over 20 hours of hands-on fully operating training, he may apply for fully operating evaluation.

5. 訓練時數達到上述之時數後，可向管理員申請考核。考核通過後，可於週一至週五8:00~17:00自行操作。全程自行操作累積使用時數達30小時以上，並未有任何違反機台規定與任何損及行為者，可申請全開放時段之使用權限。

Those who have accumulated the above-mentioned hours of training can approach the administrator for the evaluation application. Once the users pass the evaluation, they can operate the instrument independently from Monday to Friday between 8:00 AM and 5:00 PM. Those accumulating 30 hours of independent operation without violating any regulation or causing any damage may apply for unrestricted access permission.

6. 合格使用者皆有訓練新訓人員之義務。

All qualified users are obligated to train new personnel.

7. 各實驗室可自行訓練新訓人員。

Training of new personnel can be conducted voluntarily by members of each lab.

8.考核通過者若連續 6 個月無操作紀錄，取消其自行操作資格。日後若需自行操作，需另行申請、訓練、考核。

Qualified users without any record of operation for 6 months will be disqualified from independent operation. They will be required to repeat the process of application, training, and evaluation again, should they need to operate independently.

9. 本中心將於實驗完畢後依據使用時間斟酌自儲值費用中扣取實驗費用。

The charge for the operation will be deducted from the pre-paid account of your membership upon completion of experiment.

樣品規範 Sample specifications

1. 為使儀器提供給必要研究者使用，避免儀器資源的浪費，請事先與機台管理者詳細討論後，再決定是否進入機台觀察，以充分發揮本儀器之功能。

Use of instruments should be prioritized for researchers requiring the instruments. To avoid any possible waste of resources, users must discuss with the administrator before deciding whether observation is necessary. Usage of the machine should be optimized.

2.操作前必需詳細說明試片之材料種類、製作方式與溶劑種類。為減少儀器不必要的污染，本機台對於檢驗樣品的限制如下：

樣品僅限單一的固體（非粉末）。

樣品大小必須在 8mm×8mm～20mm×20mm 尺寸內，厚度 10 mm 以內。

量測範圍：700~7899 cm^-1。

注意基板材質，吸收太強或有特殊吸收峰會影響量測數據。

請事先與工程師連絡，說明所需之量測。

The material, fabrication, and solvent should be specified before operation. The following restrictions will be apply to samples in order to minimize contamination.

Samples should be in solid not powder.

Area of samples should be within the range of 8mm×8mm～20mm×20mm. Thickness of samples should be below 10 mm.

Measuring range is 700~7899 cm^-1.

Material of substrate has an influence on the results of measurements. Strong absorption peak or specific absorption peak will affect the spectrum.

Please inform and discuss with the administrator before you start the experiment.

3. 存取資料請自備隨身碟進行檔案傳輸。

Users are advised to prepare flash drive for data storage.

4. 自行操作人員，若擅自放入上述有害的試樣於本儀器者，將被吊銷操作資格。

If the qualified user is found loading any harmful sample with above-mentioned description, the user will be disqualified from operating the instrument.

5. 委託操作者上機前，技術員會再次要求確認您的樣品種類，請誠實申報。若發現申報不實，本中心將取消您的使用資格。

In cases of commissioned operation, the administrator will verify the description of the sample with you. If sample description is found to be false, you will be disqualified from using the instrument.

6. 若因違反規定造成儀器污染或損壞時，所隸屬單位及其指導教授須負責賠償，賠償費用由原廠評估，再由本中心開會決議後執行並暫停儀器之使用權。

If violation of regulation results in contamination or damage of the instrument, the institute and the advisor will bear the cost of compensation, which will be estimated by the manufacturer. We may disqualify the user from using the instrument.