高解析度 X 光繞射儀 High Resolution X-ray Diffractometer (maintenance)
聯絡方式 Contact
儀器管理者 Instrument administrator
賴良一先生Rex Lai TEL: 03-5712121 ext 55637
EMAIL: rexlai@nycu.edu.tw
對外開放服務時間 Opening hours
週一~週日 上午00:00~晚上24:00
00:00~24:00 from Monday to Sunday
使用功能說明 Applications
1. Poly-crystal s, crystal and phase identification (θ-2θ 、 Ω -2θ 、 θ scan)
2. Thin film diffraction and grazing incident x-ray diffraction
3. Powde r, bulk diffraction and rocking curve
4. Small area diffraction
規格 Specifications
1.Brand 1 ： Ital, Model IS2773-00LFF (40KV ， 50mA)
2.Sealed Tube ： 全功率 2000W
3.光學系統包含(Optical system contains)：
Soller slit、 Graphite monochromator、 Dual channel analyzer crystal 、 Double crystal (1 st and 2 nd crystal channel cut)
4.解析度(Resolution)： 5 、 12 、 25 arcsec depend on the channel cut
收費標準 Fee
1.委託操作費用(Commissioning fee )
學術單位(Academic institute) 1250元/hr
業界( Corporation) 2500元/hr
2.自行操作會員收費(independent-operation fee)
學術單位(Academic institute) 24800/40 hr，
業界( Corporation) 49600/40 hr，
3.自行操作訓練 (Training fee)
若由各單位合格操作者自行訓練，其訓練使用時數由各單位之會員時數扣除費用
若委託本中心代為訓練，費用為：
If training is conducted by a qualified operator, the charge for the training period will be deducted from the membership account of the institute. If the training is conducted by the administrator, the charge is as follows:
學術單位(Academic institute 1250/hr)
業界( Corporation 2500/hr)
管理及服務辦法 User regulations
1.本機台為B級機台，提供委託及自行操作服務。
The system is classified as a Grade B instrument, and operation can be carried out by the individual making the reservation or by qualified personnel.
2.申請委託操作者須事先與儀器管理員連絡並進行實驗討論評估，確認樣品及製程可使用本機台，並由管理員估價計算費用後，經指導教授或主管同意後，方可提出使用申請。
Those applying for commissioned operation should discuss and evaluate the experiment with the instrument administrator in advance, ensuring that the sample and fabrication process are suited for the instrument. The application can be filed after the cost is estimated by the administrator and approved by either the advisor or the supervisor.
3.委託操作使用者採序號預約，確認可提出使用申請者請先至本中心網站下載『XRD實驗申請單』，詳填資訊後，e-mail至cnst-adm@cc.nctu.edu.tw並以電話或E-mail與儀器負責人洽詢使用時段及確認實驗條件與試片製備。委託申請人需在現場共同進行實驗。
Each case of commissioned operation is by reservation only. Applicants who have been evaluated and approved can down the “ XRD application form” from our website, and email the completed form to cnst-adm@cc.nctu.edu.tw. The applicants are required to contact the instrument supervisor via phone or email regarding the available time slot, sample preparation and fabrication. The applicants have to be present for the duration of the experiment.
4.申請自行操作者，可於與儀器管理員連絡並進行實驗討論評估，確認樣品及製程可使用本機台，經指導教授或主管同意後，始可申請加入本中心會員並提出自行操作訓練考核申請，其訓練考核程序請參照『自行操作訓練與考核辦法』，通過考核後始可自行操作。
The applicant who is willing to operate the instrument by himself should discuss the details of his experiment, such as sample confirmation and fabrication, with the administrator first. After obtaining permission from the supervisor, the applicant can apply for membership of the center as well as evaluation of operation and training. For details about evaluation procedures, please refer to “VI. Guideline for independent operation and evaluation.” Those who pass the evaluation can operate the instrument independently.
5.自行操作者採取網路預約。通過機台考核之合格使用者始可取得網路預約之帳號。加入會員及申請訓練者請先至本中心網站下載『XRD實驗申請單』，詳填資訊後，e-mail至cnst-adm@cc.nctu.edu.tw並以電話或E-mail與儀器負責人洽詢訓練考核相關事宜。
The qualified users can make reservations online. After passing the practical evaluation, users can obtain an account number for online reservation purpose. Those who wish to apply for membership and training, please download the “ XRD application form” from our website. Email the completed form to cnst-adm@cc.nctu.edu.tw. Users should contact the instrument supervisor via phone or email for details regarding training and evaluation.
6.使用者須遵守實驗室所有相關規定。違反實驗室規定者依本中心實驗室管理規則辦理。
Users must abide by the regulations of the laboratory. Those in violation of lab regulations are subject to punishments accordingly.
7.。如有任何疑問，歡迎來電洽詢儀器負責人員。
Please feel free to contact the administrator for any further inquiries.
8.機台使用費用規定請參照『收費標準』。
Please refer to “Fee” for details of fees for using the instrument.
自行操作訓練與考核辦法 Guideline for independent operation and evaluation
1.本系統自行操作各單位（以指導教授、計畫主持人或公司行號為單位）開放三個名額，每位申請者須同時提出其研究使用計畫及材料特性予本中心，由本中心評估並決定是否可接受其申請。
The applicants who want to operate by themselves need to submit the details of their experiment and sample material for application of membership and the training program. The account of membership is registered under your supervisor, PI, or company name.
2. 申請者上網下載並填寫『XRD實驗申請單』詳填使用者與試片資訊後，e-mail至rexlai@nycu.edu.tw，本中心將儘速回覆您的使用申請。申請核可後，管理員會以E-mail將『見習訓練紀錄表』寄予申請人，在申請人見習時數完成後，可email與管理員洽詢上機訓練時段。
Applicants should download the “XRD application form” online and email the completed form, including details about the user and lamella, to rexlai@nycu.edu.tw. We will respond to your application as soon as possible. Once the application is approved, the administrator will email a log sheet for the probationary training to the applicant. Upon completion of probationary training, the applicant can contact the administrator for the booking of hands-on training.
3. 合格使用者皆有訓練新訓人員之義務。
All qualified users are obligated to train new personnel.
4. 各實驗室可自行訓練新訓人員。
Training of new personnel can be conducted voluntarily by members of each lab.
5. 考核通過者若連續 6 個月無操作紀錄，取消其自行操作資格。日後若需自行操作，需另行申請、訓練、考核。
Qualified users without any record of operation for 6 months will be disqualified from independent operation. They will be required to repeat the process of application, training, and evaluation again, should they need to operate independently.
6. 本中心將於實驗完畢後依據使用時間斟酌自儲值費用中扣取實驗費用。
The charge for the operation will be deducted from the pre-paid account of your membership upon completion of experiment.
樣品規範 Sample specifications
1.使儀器提供給必要研究者使用，避免儀器資源的浪費，建議與機台管理者詳細討論後，再決定是否進入機台觀察，以充分發揮本儀器之功能。
Use of instruments should be prioritized for researchers requiring the instruments. To avoid any possible waste of resources, users must discuss with the administrator before deciding whether observation is necessary. Usage of the machine should be optimized.
2. 操作前必需詳細說明試片之材料種類、製作方式與溶劑種類。
The material, fabrication, and solvent should be specified before operation.
3.存取資料請自備空白光碟片。為避免設備中毒，禁用隨身碟進行圖檔傳輸。
Users are advised to prepare CDs for data storage. The use of flash drive is forbidden to prevent any possibility of virus infection.
4. 自行操作人員，若擅自放入上述有害的試樣於本儀器者，將被吊銷操作資格。
If the qualified user is found loading any harmful sample with above-mentioned description, the user will be disqualified from operating the instrument.
5. 委託操作者上機前，技術員會再次要求確認您的樣品種類，請誠實申報。若發現申報不實，本中心將取消您的使用資格。
In cases of commissioned operation, the administrator will verify the description of the sample with you. If sample description is found to be false, you will be disqualified from using the instrument.
6. 若因違反規定造成儀器污染或損壞時，所隸屬單位及其指導教授須負責賠償，賠償費用由原廠評估，再由本中心開會決議後執行並暫停儀器之使用權。
If violation of regulation results in contamination or damage of the instrument, the institute and the advisor will bear the cost of compensation, which will be estimated by the manufacturer. We may disqualify the user from using the instrument.
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